Reacción #527809

ord-421b47c7408749a68881a84dac61fe1d

Disolventes

Condiciones de reacción

Condiciones detalladas
See reaction.notes.procedure_details.

Tratamiento posterior

  1. 1
    OtroWhen the starting materials have reacted completely

Procedimiento

A reaction mixture comprising 33 g (0.26 mol) of 2-ethylhexylamine and 50 g (0.12 mol) of 2-(4-camphylidenemethylene-anilino)-4,6-dichloro-1,3,5-triazine in toluene is heated to 90° C. in the presence of sodium acetate. When the starting materials have reacted completely, the mixture is worked up. The product (95%) is a yellow viscous oil. UV (ethanol, c=1 mg/100 ml): λmax =345 nm, E=0.57.

Fuente

DOI: 10.6084/m9.figshare.5104873.v1Patente: US05520906uspto-grants-1996_05