Reacción #52595

ord-1c489b6e3bdf42119d09d797f8064076

Disolventes

Condiciones de reacción

Condiciones detalladas
See reaction.notes.procedure_details.

Tratamiento posterior

  1. 1
    FiltraciónThe precipitate was filtered
  2. 2
    Lavadowashed with water
  3. 3
    Otrodried in a vacuum oven

Procedimiento

A mixture of 82.0 mg 5-amino-2-oxindole and 131.0 mg 4-methoxycarbonylbenzoyl chloride in pyridine was stirred at room temperature for 3 hr and poured into ice water. The precipitate was filtered, washed with water and dried in a vacuum oven to give 138.0 mg of 5-(4-methoxycarbonylbenzamido)-2oxindole (81% yield).

Fuente

DOI: 10.6084/m9.figshare.5104873.v1Patente: US06855730B2uspto-grants-2005_02