Reacción #523837

Ecuación de reacción

4-trifluoromethoxybenzoyl chloride

1,12-dodecanediamine

potassium hydroxide

→

N,N'-Dodecamethylenebis(4-trifluoromethoxybenzamide)

Disolventes

ethylene dichloride

Condiciones de reacción

Tratamiento posterior

1. 1
   Otro, was prepared as in Example 1 using 24.8 g
2. 2
   Otroof ethylene dichloride and recrystallization twice from ethanol

Procedimiento

m.p. 158°-159° C., 11.3 g., was prepared as in Example 1 using 24.8 g. of 4-trifluoromethoxybenzoyl chloride in 150 ml. of ethylene dichloride, 10.0 g. of 1,12-dodecanediamine, 60 ml. of 10% aqueous potassium hydroxide solution, 350 ml. of ethylene dichloride and recrystallization twice from ethanol and once from isopropyl alcohol.

Fuente