Reacción #5223

ord-dcadfe0e1eca4e47a8b88dad58fe8309

Reactivos

Ninguno

Disolventes

Condiciones de reacción

Condiciones detalladas
See reaction.notes.procedure_details.

Tratamiento posterior

  1. 1
    workup.STIRRINGThereafter, the mixture was stirred at room temperature for 19 hours

Procedimiento

2-Aminoethanol (13.76 g, 225.3 mmol) was dissolved in CHCl3 (750 ml). To the solution was added dropwise palmitoyl chloride (15.48 g, 56.3 mmol) with stirring under ice cooling. Thereafter, the mixture was stirred at room temperature for 19 hours.

Fuente

DOI: 10.6084/m9.figshare.5104873.v1Patente: US05243035uspto-grants-1993_09