Reacción #520225

ord-b0f16c51de7747f9ab721b7f67c9b915

Disolventes

Condiciones de reacción

Condiciones detalladas
See reaction.notes.procedure_details.

Tratamiento posterior

  1. 1
    OtroThe solvents were removed in vacuo
  2. 2
    Otrothe resulting colourless oil was purified by column chromatography (ethyl acetate) on silica

Procedimiento

Compound 3 (11.6 g, 38 mmol) in ethanol (200 ml) and aqueous ammonia (50 ml) was stirred overnight. The solvents were removed in vacuo and the resulting colourless oil was purified by column chromatography (ethyl acetate) on silica.

Fuente

DOI: 10.6084/m9.figshare.5104873.v1Patente: US06666989B1uspto-grants-2003_12