Reacción #520225
ord-b0f16c51de7747f9ab721b7f67c9b915
Ecuación de reacción
Reactivos
Ninguno
Condiciones de reacción
Condiciones detalladas
See reaction.notes.procedure_details.
Tratamiento posterior
- 1OtroThe solvents were removed in vacuo
- 2Otrothe resulting colourless oil was purified by column chromatography (ethyl acetate) on silica
Procedimiento
Compound 3 (11.6 g, 38 mmol) in ethanol (200 ml) and aqueous ammonia (50 ml) was stirred overnight. The solvents were removed in vacuo and the resulting colourless oil was purified by column chromatography (ethyl acetate) on silica.