Reacción #518098

Ecuación de reacción

piperazine

9-anthacenemethanol

pyridine

p-nitrophenyl chloroformate

→

9-anthracenylmethyl-1-piperazinecarboxylate

Disolventes

water

Condiciones de reacción

Tratamiento posterior

1. 1
   OtroProduct is isolated
2. 2
   Otroto provide a crude anthrylmethyl p-nitrophenyl carbonate, which
3. 3
   Extracciónextracted with a solvent
4. 4
   LavadoThe product is washed
5. 5
   Otrodried

Procedimiento

PAC is produced by adding 9-anthacenemethanol and pyridine to a solution of p-nitrophenyl chloroformate. Product is isolated to provide a crude anthrylmethyl p-nitrophenyl carbonate, which is then added to a solution of piperazine. The reacted mixture is poured into water and extracted with a solvent, preferably an organic solvent such as toluene. The product is washed and dried to provide 9-anthracenylmethyl-1-piperazinecarboxylate (PAC).

Fuente