Reacción #50870

Ecuación de reacción

3-bromothiophenol

potassium carbonate

iodomethane

→

title compound

3-(methylthio)phenylbromide

Disolventes

acetone

Condiciones de reacción

Tratamiento posterior

1. 1
   TemperaturaThe heterogenous mixture was refluxed for 4 hrs
2. 2
   Filtraciónfiltered
3. 3
   Concentraciónconcentrated under reduced pressure
4. 4
   workup.ADDITIONEther (200 mL) was added
5. 5
   Filtraciónthe mixture was filtered again
6. 6
   Otrofinally evaporated to dryness

Procedimiento

To a solution of 3-bromothiophenol (10 g) in acetone (250 mL) was added potassium carbonate (14.6 g) and iodomethane (4.28 mL). The heterogenous mixture was refluxed for 4 hrs., cooled to room temperature, filtered, and concentrated under reduced pressure. Ether (200 mL) was added, and the mixture was filtered again and finally evaporated to dryness to yield the title compound.

Fuente