Reacción #50163

Ecuación de reacción

benzo 15-crown-5 ether

trifluoroacetic acid

→

4'-formylbenzo-15-crown-5-ether

Condiciones de reacción

Tratamiento posterior

1. 1
   Temperaturathe mixture was heated
2. 2
   Temperaturato reflux for 12 hours

Procedimiento

A solution of hexamethylenetretramine (1.87 mmol, 0.27 g) in trifluoroacetic acid (1.4 cm3) was added to benzo 15-crown-5 ether (1.87 mmol, 0.5 g) under nitrogen; the mixture was heated to reflux for 12 hours.

Fuente