Reacción #50075

ord-13e21a51e5c14dccb7902b3e0d8e2a67

Ecuación de reacción

O=C1NC(=O)c2ccccc21.[K]
Potassium phthalimide
BrCCCCCCCCBr
1,8-dibromooctane
O=C1NC(=O)c2c(CCCCCCCCBr)cccc21
8-bromooctylphthalimide

Reactivos

Ninguno

Condiciones de reacción

Condiciones detalladas
See reaction.notes.procedure_details.

Tratamiento posterior

  1. 1
    Temperaturaheated to 80° C. approx.
  2. 2
    OtroReaction times and process as per Example 4

Procedimiento

Potassium phthalimide (5.4 mmoles) was added to a solution of 1,8-dibromooctane (4.41 g; 16.2 mmoles) in dimethylformamide (8 ml) and heated to 80° C. approx. under stirring. Reaction times and process as per Example 4.

Fuente

DOI: 10.6084/m9.figshare.5104873.v1Patente: US05424451uspto-grants-1995_06