Reacción #49903

Ecuación de reacción

S-(thiobenzoyl)thioglycolic acid

t-butyl hydrazine hydrochloride

Water

→

N'-t-butyl-N-(thiobenzoyl)hydrazine

Disolventes

pyridine

Condiciones de reacción

Tratamiento posterior

1. 1
   Extracciónthe mixture was extracted with ether
2. 2
   SecadoThe organic extracts were dried over anhydrous magnesium sulfate
3. 3
   Filtraciónfiltered
4. 4
   Otroevaporated

Procedimiento

S-(thiobenzoyl)thioglycolic acid (3.0 g) was dissolved in 20 ml pyridine, treated with t-butyl hydrazine hydrochloride (excess, ca. 4 g) and then was heated at ca. 120° C. for 14 hours. Water (120 ml) was added and the mixture was extracted with ether. The organic extracts were dried over anhydrous magnesium sulfate, filtered and evaporated to give crude N'-t-butyl-N-(thiobenzoyl)hydrazine as a viscous yellow oil.

Fuente