Reacción #4927

ord-020326b1e4574d44986493bf5d683e46

Ecuación de reacción

CN1CC(CCCl)Oc2ncccc2C1=S
2-(2-Chloroethyl)-2,3-dihydro-4-methylpyrido[3,2-f][1,4]-oxazepine-5(4H)-thione
CCNCC
diethylamine
→
CCN(CC)CCC1CN(C)C(=S)c2cccnc2O1
title compound
CCN(CC)CCC1CN(C)C(=S)c2cccnc2O1
2-[2-(Diethylamino)ethyl]-2,3-dihydro-4-methylpyrido[3,2-f][1,4]oxazepine-5(4H)-thione

Reactantes

CN1CC(CCCl)Oc2ncccc2C1=S
2-(2-Chloroethyl)-2,3-dihydro-4-methylpyrido[3,2-f][1,4]-oxazepine-5(4H)-thione
CCNCC
diethylamine

Reactivos

Ninguno

Disolventes

CCO
ethanol

Condiciones de reacción

Condiciones detalladas
See reaction.notes.procedure_details.

Procedimiento

2-(2-Chloroethyl)-2,3-dihydro-4-methylpyrido[3,2-f][1,4]-oxazepine-5(4H)-thione and diethylamine in ethanol are heated together to obtain the title compound.

Fuente

DOI: 10.6084/m9.figshare.5104873.v1Patente: US04727152uspto-grants-1988_02