Reacción #483047

ord-126596f24f87442ea37f8ea43d8fd9de

Ecuación de reacción

O=C(O)CCCC[C@@H]1CCSS1
lipoic acid
Cl.N=C(Nc1ccc(NC(=O)CCCCC2CCSS2)cc1)c1cccs1
compound 1
Cl.N=C(Nc1ccc(NC(=O)CCCCC2CCSS2)cc1)c1cccs1
N-(4-[[(2-Thienyl)(imino)methyl]amino]phenyl}-1,2-dithiolane-3-pentanamide Hydrochloride
O=C(O)C[C@@H]1CCSS1
trisnorlipoic acid
O=C(O)CC1CCSS1
2-(1,2-dithiolan-3-yl)acetic acid
NC(=Nc1ccc(NC(=O)CC2CCSS2)cc1)c1cccs1
N-(4-{[Amino(2-thienyl)methylidene]amino}phenyl)-2-(1,2-dithiolan-3-yl)acetamide

Condiciones de reacción

Condiciones detalladas
See reaction.notes.procedure_details.

Procedimiento

The experimental protocol used is the same as that described for compound 1, with trisnorlipoic acid [or 2-(1,2-dithiolan-3-yl)acetic acid] (prepared according to Tetrahedron Letters, (1997), 38, 33, 5785) replacing lipoic acid. Yellow foam.

Fuente

DOI: 10.6084/m9.figshare.5104873.v1Patente: US06605637B1uspto-grants-2003_08