Reacción #476184

ord-05054416c02248f89e5b132dca5599b6

Disolventes

Condiciones de reacción

Condiciones detalladas
See reaction.notes.procedure_details.

Tratamiento posterior

  1. 1
    OtroThe compound was prepared
  2. 2
    workup.ADDITIONwas added
  3. 3
    OtroThe product was recovered essentially as in Preparatory Example 1

Procedimiento

The compound was prepared using essentially the procedure of Preparatory Example 1 with 2-hydroxy biphenyl (40 g.), water (250 g.), sodium iodide (3.5 g.) and sodium hydroxide (37.6 g. of 50% in water). This mixture was heated to 100° C. with agitation and 8-chloro-1-octanol (77.4 g.) was added. The product was recovered essentially as in Preparatory Example 1.

Fuente

DOI: 10.6084/m9.figshare.5104873.v1Patente: US08378046B2uspto-grants-2013_02