Reacción #470367

Ecuación de reacción

Methoxymethylpyrrolidine

dimethyl carbonate

→

desired product

Rendimiento 60.0%

N-Methoxymethyl-N-Methylpyrrolidinium Methyl carbonate

Rendimiento 60.0%

Condiciones de reacción

Tratamiento posterior

1. 1
   Otroreacted at 120° C. for 24 hours
2. 2
   FiltraciónThe resulting solids were filtered off
3. 3
   Lavadowashed with dimethyl carbonate
4. 4
   OtroThe solids were dried in a vacuum

Procedimiento

Methoxymethylpyrrolidine (10.00 g) and 117.39 g of dimethyl carbonate were placed into an autoclave and reacted at 120° C. for 24 hours. The resulting solids were filtered off and washed with dimethyl carbonate. The solids were dried in a vacuum, giving 10.70 g of the desired product.

Fuente