Reacción #452433

Ecuación de reacción

4-dimethylamino-1-cyclohexanone ethylene ketal

→

title compound

Rendimiento 100.0%

4-dimethylamino-1-cyclohexanone

Rendimiento 100.0%

Disolventes

formic acid

Condiciones de reacción

Tratamiento posterior

1. 1
   Temperaturaat reflux for 18 hours
2. 2
   TemperaturaThe reaction mixture was then cooled to ambient and the volatiles
3. 3
   Otroremoved under reduced pressure

Procedimiento

4.96 gm (26.8 mMol) 4-dimethylamino-1-cyclohexanone ethylene ketal were dissolved in 50 mL formic acid and the solution stirred at reflux for 18 hours. The reaction mixture was then cooled to ambient and the volatiles removed under reduced pressure to give 3.78 gm (100%) of the title compound.

Fuente