Reacción #446707

Ecuación de reacción

2-aminobenzamide

benzoyl isothiocyanate

→

desired product

Rendimiento 95.0%

N-[[[2-(Aminocarbonyl)phenyl]amino]thioxomethyl)benzamide

Rendimiento 95.0%

Disolventes

ether

ether

Condiciones de reacción

Tratamiento posterior

1. 1
   workup.ADDITIONWas added dropwise
2. 2
   Otrothe solid Was collected

Procedimiento

To a stirred mixture of 13.6 g of 2-aminobenzamide and 200 ml of ether Was added dropwise, a solution of 16.3 g of benzoyl isothiocyanate in 100 ml of ether over 30 minutes. After standing 48 hours, the solid Was collected, giving 28.4 g of the desired product as grey crystals, mp 190°-192° C.

Fuente