Reacción #443147

ord-1db09a5e0cad40ed9f47361e6597ad7c

Ecuación de reacción

CC(=O)Nc1cccc2c1C(=O)C(NC(C)=O)CCC2
( 3 )
CC(=O)Nc1cccc2c1C(=O)C(NC(C)=O)CCC2
1,8-Diacetylamino-6,7,8,9-tetrahydro-5H-benzocycloheptene-9-one
CC(=O)Nc1cccc2c1C(=O)C(NC(C)=O)CC2
2,8-diacetylamino-1-tetralone
→
CC(=O)NC1CCCc2cccc(N)c2C1=O
title compound
CC(=O)NC1CCCc2cccc(N)c2C1=O
8-Acetylamino-1-amino-6,7,8,9-tetrahydro-5H-benzocycloheptene-9-one

Reactantes

—
compound
CC(=O)Nc1cccc2c1C(=O)C(NC(C)=O)CCC2
( 3 )
CC(=O)Nc1cccc2c1C(=O)C(NC(C)=O)CCC2
1,8-Diacetylamino-6,7,8,9-tetrahydro-5H-benzocycloheptene-9-one
CC(=O)Nc1cccc2c1C(=O)C(NC(C)=O)CC2
2,8-diacetylamino-1-tetralone

Reactivos

Ninguno

Condiciones de reacción

Condiciones detalladas
See reaction.notes.procedure_details.

Tratamiento posterior

  1. 1
    workup.ADDITIONThe product was post-treated

Procedimiento

The reaction was carried out in the same manner as in Example 1-(4), except that 115 mg of the compound prepared in (3) above was used instead of 2,8-diacetylamino-1-tetralone of Example 1-(4). The product was post-treated to produce 90 mg of the title compound.

Fuente

DOI: 10.6084/m9.figshare.5104873.v1Patente: US05834476uspto-grants-1998_11