Reacción #443141

ord-903fbd959e844242b7c71f59ac23c1b7

Ecuación de reacción

CC(=O)Nc1ccc(C)c2c1C(=O)C(=NO)CN2C(C)=O
( 2 )
CC(=O)Nc1ccc(C)c2c1C(=O)C(=NO)CN2C(C)=O
1-Acetyl-5-acetylamino-3-hydroxyimino-8-methyl-2,3-dihydroquinoline-4-one
CC(=O)Nc1cccc2c1C(=O)C(=NO)CC2
8-acetylamino-2-hydroxyimino-1-tetralone
→
CC(=O)Nc1ccc(C)c2c1C(=O)C(NC(C)=O)CN2C(C)=O
title compound
CC(=O)Nc1ccc(C)c2c1C(=O)C(NC(C)=O)CN2C(C)=O
1-Acetyl-3,5-diacetylamino-8-methyl-2,3-dihydro-quinoline-4-one

Reactantes

—
compound
CC(=O)Nc1ccc(C)c2c1C(=O)C(=NO)CN2C(C)=O
( 2 )
CC(=O)Nc1ccc(C)c2c1C(=O)C(=NO)CN2C(C)=O
1-Acetyl-5-acetylamino-3-hydroxyimino-8-methyl-2,3-dihydroquinoline-4-one
CC(=O)Nc1cccc2c1C(=O)C(=NO)CC2
8-acetylamino-2-hydroxyimino-1-tetralone

Reactivos

Ninguno

Condiciones de reacción

Condiciones detalladas
See reaction.notes.procedure_details.

Tratamiento posterior

  1. 1
    workup.ADDITIONThe reaction product was post-treated

Procedimiento

The procedure of Example 1-(3) was followed by using 2.89 gm of the compound prepared in (2) above instead of 8-acetylamino-2-hydroxyimino-1-tetralone. The reaction product was post-treated to obtain 1.65 gm of the title compound.

Fuente

DOI: 10.6084/m9.figshare.5104873.v1Patente: US05834476uspto-grants-1998_11