Reacción #443130

ord-ddb8a75db33c4e88b995616723b16b86

Ecuación de reacción

COc1ccc(NC(C)=O)c2c1CCC(NC(C)=O)C2=O
( 2 )
COc1ccc(NC(C)=O)c2c1CCC(NC(C)=O)C2=O
2,8-Diacetylamino-5-methoxy-1-tetralone
CC(=O)Nc1cccc2c1C(=O)C(NC(C)=O)CC2
2,8-diacetylamino-1-tetralone
→
COc1ccc(N)c2c1CCC(NC(C)=O)C2=O
title compound
COc1ccc(N)c2c1CCC(NC(C)=O)C2=O
2-Acetylamino-8-amino-5-methoxy-1-tetralone

Reactantes

—
compound
COc1ccc(NC(C)=O)c2c1CCC(NC(C)=O)C2=O
( 2 )
COc1ccc(NC(C)=O)c2c1CCC(NC(C)=O)C2=O
2,8-Diacetylamino-5-methoxy-1-tetralone
CC(=O)Nc1cccc2c1C(=O)C(NC(C)=O)CC2
2,8-diacetylamino-1-tetralone

Reactivos

Ninguno

Condiciones de reacción

Condiciones detalladas
See reaction.notes.procedure_details.

Procedimiento

The same procedure as in Example 1-(4) was carried out, except that 200 mg of the compound prepared in (2) above was used instead of 2,8-diacetylamino-1-tetralone. Upon the post-treatment in the same manner as in Example 1-(4), 130 mg of the title compound was obtained.

Fuente

DOI: 10.6084/m9.figshare.5104873.v1Patente: US05834476uspto-grants-1998_11