Reacción #438668

Ecuación de reacción

methyl acrylate

2-methoxyethylamine

acrylonitrile

→

methyl N-(2-cyanoethyl)-N-(2-methoxyethyl)-3-aminopropionate

Condiciones de reacción

Tratamiento posterior

1. 1
   ConcentraciónVacuum concentration

Procedimiento

At 20 to 30° C., 11.4 g of methyl acrylate was added to 10.0 g of 2-methoxyethylamine, which was allowed to stand for 2 hours. Then 15.0 g of acrylonitrile was added to the reaction solution, which was heated at 70° C. for 20 hours. Vacuum concentration yielded methyl N-(2-cyanoethyl)-N-(2-methoxyethyl)-3-aminopropionate.

Fuente