Reacción #43812

ord-7127dda99fa6496f990591c54edd8f2f

Disolventes

Condiciones de reacción

Condiciones detalladas
See reaction.notes.procedure_details.

Tratamiento posterior

  1. 1
    ConcentraciónThe reaction was concentrated

Procedimiento

The product of example 25, step d.) (140 mg, 0.359 mmol) was stirred in 4 M HCl in dioxane (1 mL) at ambient temperature for an hour. The reaction was concentrated to give the sub-title compound that was used in crude form without purification. MS: ESI (positive): 290 (M+H).

Fuente

DOI: 10.6084/m9.figshare.5104873.v1Patente: US07732618B2uspto-grants-2010_06