Reacción #428903

ord-b4192dcde92244599637877ecfda0137

Condiciones de reacción

Condiciones detalladas
See reaction.notes.procedure_details.

Procedimiento

Reaction between 500 grams of isophorone diisocyanate and 62.6 grams of cyclohexyl isocyanate was effected in the presence of 5.63 grams of a carbodiimidizing catalyst (3methyl-1-phenyl-2-phospholene-1-oxide) at 180° C. for 24 hours, yielding isophorone carbodiimide having a degree of polymerization of 10. The carbodiimide resin was thoroughly pulverized. To 200 grams of this carbodiimide, 200 grams of distilled water having 1 gram of a nonylphenyl nonionic surfactant (Nonypol) dissolved therein was slowly added, obtaining a carbodiimide dispersion (resin concentration 50% by weight).

Fuente

DOI: 10.6084/m9.figshare.5104873.v1Patente: US05856014uspto-grants-1999_01