Reacción #42146

ord-0b6a244a31ae4bdea68240493807b244

Ecuación de reacción

CCCCP(CCCC)CCCC
Tri-n-butylphosphine
Cl
hydrochloric acid
[Na+].c1ccc([B-](c2ccccc2)(c2ccccc2)c2ccccc2)cc1
sodium tetraphenylborate
→
CCCC[PH+](CCCC)CCCC.c1ccc([B-](c2ccccc2)(c2ccccc2)c2ccccc2)cc1
tri-n-butylphosphonium tetraphenylborate
Rendimiento 53.0%

Reactantes

CCCCP(CCCC)CCCC
Tri-n-butylphosphine
Cl
hydrochloric acid
[Na+].c1ccc([B-](c2ccccc2)(c2ccccc2)c2ccccc2)cc1
sodium tetraphenylborate

Reactivos

Ninguno

Condiciones de reacción

Condiciones detalladas
See reaction.notes.procedure_details.

Procedimiento

Tri-n-butylphosphine is reacted with hydrochloric acid in the presence of sodium tetraphenylborate to produce tri-n-butylphosphonium tetraphenylborate (53% yield) (see Nonpatent Document 6).

Fuente

DOI: 10.6084/m9.figshare.5104873.v1Patente: US07728176B2uspto-grants-2010_06