Reacción #42144

ord-26bcb57d0e5a476a8aaa17b3207a4354

Condiciones de reacción

Condiciones detalladas
See reaction.notes.procedure_details.

Procedimiento

Tricyclohexylphosphine is reacted with fluoroboric acid to synthesize tricyclohexylphosphonium tetrafluoroborate, which is reacted with sodium tetraphenylborate to produce tricyclohexylphosphonium tetraphenylborate (75% yield). A similar process is described in which tri-tert-butylphosphine is used as starting material to produce tri-tert-butylphosphonium tetraphenylborate (71% yield) (see Nonpatent Document 4).

Fuente

DOI: 10.6084/m9.figshare.5104873.v1Patente: US07728176B2uspto-grants-2010_06