Reacción #42011

ord-c891a9a360914f4b89c8c19dfb2ab01a

Disolventes

Condiciones de reacción

Condiciones detalladas
See reaction.notes.procedure_details.

Tratamiento posterior

  1. 1
    Temperaturawas refluxed
  2. 2
    workup.ADDITIONwas added
  3. 3
    Filtraciónthe catalyst was filtered off
  4. 4
    Concentraciónconcentrated

Procedimiento

A mixture containing Catalyst A or B (0.05 g) and ethyl oleate (1.55 g, 5 mmol) and pentanol (10 ml) was refluxed with stirring for 40 h. On cooling ether (30 ml) was added and the catalyst was filtered off. The organic washings were combined and concentrated to give pentyl oleate as an oil (1.6 g, 91% yield).

Fuente

DOI: 10.6084/m9.figshare.5104873.v1Patente: US07728159B2uspto-grants-2010_06