Reacción #417924

Ecuación de reacción

sodium hydroxide

29

methyl 2-(undec-4Z-enyloxy)benzoate

→

yellow oil

Rendimiento 99.5%

2-(undec-4Z-enyloxy)benzoic acid

Rendimiento 99.5%

Disolventes

methanol

Condiciones de reacción

Tratamiento posterior

1. 1
   TemperaturaThe solution is refluxed for 24 hours
2. 2
   OtroAfter evaporating off the solvent
3. 3
   Extracciónextracted with DCM

Procedimiento

500 μL of 1 N sodium hydroxide solution (500 μmol) are added portionwise to 80 mg of 29 (263 μmol) in methanol (3 mL). The solution is refluxed for 24 hours. After evaporating off the solvent, the reaction medium is acidified with 0.5 N HCl and extracted with DCM. 76 mg of a yellow oil are obtained, i.e. a yield of 99%.

Fuente