Reacción #411324

ord-4ec6c7557f71461d85c514093cfbb975

Condiciones de reacción

Condiciones detalladas
See reaction.notes.procedure_details.

Tratamiento posterior

  1. 1
    Otroto dry at ambient temperature for approximately 20 minutes
  2. 2
    TemperaturaThe painted titanium substrate was subsequently heat
  3. 3
    workup.ADDITIONtreated in a furnace
  4. 4
    Otroat approximately 500° C.
  5. 5
    Otrofor approximately 20-30 minutes

Procedimiento

After the titanium substrate surface was roughened, it was painted with a n-butanol solution containing salts of iridium and tantalum in a ratio of iridium to tantalum of approximately 65% to 35% by weight. The applied solution was allowed to dry at ambient temperature for approximately 20 minutes. The painted titanium substrate was subsequently heat treated in a furnace having an oxygen containing atmosphere at approximately 500° C. for approximately 20-30 minutes to form an iridium oxide/tantalum oxide composite coating. The process of painting and heat treating the titanium substrate was repeated in order to obtain a total loading of about 2.0 g/m2. After this loading was achieved, the painted substrate was heat treated for approximately one hour at approximately 500° C.

Fuente

DOI: 10.6084/m9.figshare.5104873.v1Patente: US06217729B1uspto-grants-2001_04