Reacción #409789

ord-e7704ad5b6424d6fa7f7110fcbae96b8

Ecuación de reacción

[Al+3].[Al+3].[O-2].[O-2].[O-2]
aluminum oxide
[Al+3].[Al+3].[O-2].[O-2].[O-2]
aluminum oxide
CCOC(=O)CCCC[c-]1cccc1.[Fe+2].c1cc[cH-]c1
III
CCOC(=O)CCCC[c-]1cccc1.[Fe+2].c1cc[cH-]c1
5-Ferrocenylpentanoic Acid Ethyl Ester
→
OCCCCC[c-]1cccc1.[Fe+2].c1cc[cH-]c1
5-Ferrocenylpentanol

Reactantes

[Al+3].[Al+3].[O-2].[O-2].[O-2]
aluminum oxide
[Al+3].[Al+3].[O-2].[O-2].[O-2]
aluminum oxide
CCOC(=O)CCCC[c-]1cccc1.[Fe+2].c1cc[cH-]c1
III
CCOC(=O)CCCC[c-]1cccc1.[Fe+2].c1cc[cH-]c1
5-Ferrocenylpentanoic Acid Ethyl Ester

Reactivos

Ninguno

Disolventes

ClCCl
CH2Cl2
ClCCl
CH2Cl2

Condiciones de reacción

Condiciones detalladas
See reaction.notes.procedure_details.

Procedimiento

Yield: 378 mg (89% of the theoretical) TLC: Rf (aluminum oxide, CH2Cl2)=0.2 Column chromatography: aluminum oxide, neutr. (act. III), CH2Cl2

Fuente

DOI: 10.6084/m9.figshare.5104873.v1Patente: US06211356B1uspto-grants-2001_04