Reacción #3824

Ecuación de reacción

2,2'-dithiobisbenzoyl chloride

4-iodoaniline

→

title compound

Rendimiento 36.0%

2,2'-dithiobis[N-(4-iodophenyl)benzamide]

Rendimiento 36.0%

Disolventes

pyridine

dichloromethane

Condiciones de reacción

Tratamiento posterior

1. 1
   OtroThis compound was prepared
2. 2
   OtroThe crude product was recrystallized from water-DMF

Procedimiento

This compound was prepared according to the general method of Example 77 using 2,2'-dithiobisbenzoyl chloride (2.00 g, 5.83 mmol) in 50 mL of dichloromethane and 4-iodoaniline (2.54 g, 11.6 mmol) in 20 mL of pyridine. The crude product was recrystallized from water-DMF to yield 1.48 g of the title compound, mp 268°-271° C. (dec.).

Fuente