Reacción #3822

Ecuación de reacción

2,2'-dithiobisbenzoyl chloride

4-aminophenyl methyl sulfone

→

title compound

Rendimiento 56.0%

2,2'-Dithiobis[N-[4-(methylsulfonyl)phenyl]benzamide]

Rendimiento 56.0%

Disolventes

pyridine

dichloromethane

Condiciones de reacción

Tratamiento posterior

1. 1
   OtroThis compound was prepared
2. 2
   OtroThe crude product was recrystallized from acetonitrile-DMF

Procedimiento

This compound was prepared according to the general method of Example 77 using 2,2'-dithiobisbenzoyl chloride (2.00 g, 5.83 mmol) in 50 mL of dichloromethane and 4-aminophenyl methyl sulfone (2.00 g, 11.7 mmol) in 16 mL of pyridine. The crude product was recrystallized from acetonitrile-DMF to yield 2.0 g of the title compound, mp 236°-238° C.

Fuente