Reacción #3819

Ecuación de reacción

2,2'-dithiobisbenzoyl chloride

4-aminobenzotrifluoride

→

title compound

Rendimiento 24.3%

2,2'-Dithiobis[N-[4-(trifluoromethyl)phenyl]benzamide]

Rendimiento 24.3%

Disolventes

pyridine

dichloromethane

Condiciones de reacción

Tratamiento posterior

1. 1
   OtroThis compound was prepared
2. 2
   OtroThe crude product was recrystallized from water-DMF

Procedimiento

This compound was prepared according to the general method of Example 77 using 2,2'-dithiobisbenzoyl chloride (1.12 g, 3.26 mmol) in 25 mL of dichloromethane and 4-aminobenzotrifluoride (1.05 g, 6.53 mmol) in 8 mL of pyridine. The crude product was recrystallized from water-DMF to yield 0.47 g of the title compound, mp 272°-275° C.

Fuente