Reacción #3816

Ecuación de reacción

2,2'-dithiobisbenzoyl chloride

3-aminobenzotrifluoride

→

title compound

Rendimiento 15.1%

2,2'-Dithiobis[N-[3-(trifluoromethyl)phenyl]benzamide]

Rendimiento 15.1%

Disolventes

pyridine

dichloromethane

Condiciones de reacción

Tratamiento posterior

1. 1
   OtroThis compound was prepared
2. 2
   OtroThe crude product was recrystallized from ethanol

Procedimiento

This compound was prepared according to the general method of Example 77 using 2,2'-dithiobisbenzoyl chloride (2.00 g, 5.83 mmol) in 50 mL of dichloromethane and 3-aminobenzotrifluoride (1.87 g, 11.6 mmol) in 15 mL of pyridine. The crude product was recrystallized from ethanol, then ethyl ether to yield 0.519 g of the title compound, mp 167°-168° C.

Fuente