Reacción #3813

Ecuación de reacción

2,2'-dithiobisbenzoyl chloride

3,4-dimethylaniline

→

title compound

Rendimiento 16.8%

2,2'-Dithiobis[N-(3,4-dimethylphenyl)benzamide]

Rendimiento 16.8%

Disolventes

pyridine

dichloromethane

Condiciones de reacción

Tratamiento posterior

1. 1
   OtroThis compound was prepared
2. 2
   OtroThe crude product was triturated with ethyl ether
3. 3
   Filtraciónfiltered

Procedimiento

This compound was prepared according to the general method of Example 77 using 2,2'-dithiobisbenzoyl chloride (1.12 g, 3.26 mmol) in 25 mL of dichloromethane and 3,4-dimethylaniline (0.79 g, 6.52 mmol) in 8 mL of pyridine. The crude product was triturated with ethyl ether and filtered to yield 0.28 g of the title compound, mp 224°-227° C.

Fuente