Reacción #3811

Ecuación de reacción

2,2'-dithiobisbenzoyl chloride

3,4-dichloroaniline

→

title compound

Rendimiento 10.2%

2,2'-Dithiobis[N-(3,4-dichlorophenyl)benzamide]

Rendimiento 10.2%

Disolventes

pyridine

dichloromethane

Condiciones de reacción

Tratamiento posterior

1. 1
   OtroThis compound was prepared
2. 2
   OtroThe crude product was recrystallized from ethyl acetate-hexanes

Procedimiento

This compound was prepared according to the general method of Example 77 using 2,2'-dithiobisbenzoyl chloride (1.04 g, 3.03 mmol) in 25 mL of dichloromethane and 3,4-dichloroaniline (0.982 g, 6.06 mmol) in 8 mL of pyridine. The crude product was recrystallized from ethyl acetate-hexanes to yield 0.184 g of the title compound, mp 230°-233° C.

Fuente