Reacción #3810

Ecuación de reacción

2,2'-dithiobisbenzoyl chloride

3,5-bis(trifluoromethyl)aniline

→

title compound

Rendimiento 8.0%

2,2'-Dithiobis[N-[3,5-bis(trifluoromethyl)phenyl]benzamide]

Rendimiento 8.0%

Disolventes

pyridine

dichloromethane

Condiciones de reacción

Tratamiento posterior

1. 1
   OtroThis compound was prepared
2. 2
   OtroThe crude product was recrystallized from ethyl acetate-hexanes (1:9)

Procedimiento

This compound was prepared according to the general method of Example 77 using 2,2'-dithiobisbenzoyl chloride (2.00 g, 5.83 mmol) in 50 mL of dichloromethane and 3,5-bis(trifluoromethyl)aniline (2.66 g, 11.6 mmol) in 21 mL of pyridine. The crude product was recrystallized from ethyl acetate-hexanes (1:9) to yield 0.34 g of the title compound, mp 213°-214° C.

Fuente