Reacción #3807

Ecuación de reacción

2,2'-dithiobisbenzoyl chloride

m-toluidine

→

title compound

Rendimiento 42.0%

2,2'-Dithiobis[N-(3-methylphenyl)benzamide]

Rendimiento 42.0%

Disolventes

pyridine

dichloromethane

Condiciones de reacción

Tratamiento posterior

1. 1
   OtroThis compound was prepared
2. 2
   OtroThe crude product was recrystallized from ethyl ether-ethyl acetate

Procedimiento

This compound was prepared according to the general method of Example 77 using 2,2'-dithiobisbenzoyl chloride (2.00 g, 5.83 mmol) in 50 mL of dichloromethane and m-toluidine (1.24 g, 11.6 mmol) in 10 mL of pyridine. The crude product was recrystallized from ethyl ether-ethyl acetate to yield 1.18 g of the title compound, mp 193°-195° C.

Fuente