Reacción #367730

Ecuación de reacción

sodium hydroxide

methyl alcohol

4-Bromo-2-benzoyl-isonicotinanilide

ethyl alcohol

potassium hydroxide

→

titled compound

Rendimiento 80.0%

4-Bromo-2-benzoyl-isonicotinanilide dimethyl ketal

Rendimiento 80.0%

Condiciones de reacción

Procedimiento

4-Bromo-2-benzoyl-isonicotinanilide (12.7 g) was treated as in Synthesis 11 except that ethyl alcohol was replaced by methyl alcohol and potassium hydroxide by sodium hydroxide (3 g). The titled compound was obtained in an amount of 11.4 g (yield: 80%). m.p. 189°-190° C.

Fuente