Reacción #366620

Ecuación de reacción

15-crown-5

phenylchloroformate

sodium fluoride

→

Phenylfluoroformate

Disolventes

acetonitrile

Condiciones de reacción

Tratamiento posterior

1. 1
   OtroReaction completion

Procedimiento

To a solution of phenylchloroformate in acetonitrile is charged sodium fluoride. To this mixture is charged the 15-crown-5(“15C5”) at ambient temperature. The reaction mixture is then heated to 40° C. for approximately 16 hrs. Reaction completion is monitored by gas chromatography (“G.C.”).

Fuente