Reacción #359513

ord-6960dc0b00f24868b8b73d9ea56e8cce

Ecuación de reacción

Cc1c(C)c(N2C(=O)c3ccccc3C2=O)c(C)c2c1OC(C)(C)C2c1ccc(C(C)C)cc1
2-[3-(4-isopropylphenyl)-2,2,4,6,7-pentamethyl-2,3-dihydro-1-benzofuran-5-yl]-1H-isoindole-1,3(2H)-dione
→
Cc1c(C)c(N2Cc3ccccc3C2)c(C)c2c1OC(C)(C)C2c1ccc(C(C)C)cc1
title compound
Rendimiento 57.0%
Cc1c(C)c(N2Cc3ccccc3C2)c(C)c2c1OC(C)(C)C2c1ccc(C(C)C)cc1
2-[3-(4-Isopropylphenyl)-2,2,4,6,7-pentamethyl-2,3-dihydro-1-benzofuran-5-yl]isoindoline
Rendimiento 57.0%

Reactantes

Cc1c(C)c(N2C(=O)c3ccccc3C2=O)c(C)c2c1OC(C)(C)C2c1ccc(C(C)C)cc1
2-[3-(4-isopropylphenyl)-2,2,4,6,7-pentamethyl-2,3-dihydro-1-benzofuran-5-yl]-1H-isoindole-1,3(2H)-dione

Reactivos

Ninguno

Disolventes

CCCCCC
Hexane

Condiciones de reacción

Condiciones detalladas
See reaction.notes.procedure_details.

Procedimiento

By using 2-[3-(4-isopropylphenyl)-2,2,4,6,7-pentamethyl-2,3-dihydro-1-benzofuran-5-yl]-1H-isoindole-1,3(2H)-dione, the title compound was synthesized according to Example 2a. Yield: 57%. Melting point: 113-114° C. (Hexane)

Fuente

DOI: 10.6084/m9.figshare.5104873.v1Patente: US07456162B2uspto-grants-2008_11