Reacción #359509

ord-3772576513c843e5b58b41fc16152e0d

Ecuación de reacción

Cc1ccc(C2c3c(C)c(N4C(=O)c5ccccc5C4=O)c(C)c(C)c3OC2(C)C)cc1
2-[2,2,4,6,7-pentamethyl-3-(4-methylphenyl)-2,3-dihydro-1-benzofuran-5-yl]-1H-isoindole-1,3(2H)-dione
→
Cc1ccc(C2c3c(C)c(N4Cc5ccccc5C4)c(C)c(C)c3OC2(C)C)cc1
title compound
Rendimiento 46.0%
Cc1ccc(C2c3c(C)c(N4Cc5ccccc5C4)c(C)c(C)c3OC2(C)C)cc1
2-[2,2,4,6,7-Pentamethyl-3-(4-methylphenyl)-2,3-dihydro-1-benzofuran-5-yl]isoindoline
Rendimiento 46.0%

Reactantes

Cc1ccc(C2c3c(C)c(N4C(=O)c5ccccc5C4=O)c(C)c(C)c3OC2(C)C)cc1
2-[2,2,4,6,7-pentamethyl-3-(4-methylphenyl)-2,3-dihydro-1-benzofuran-5-yl]-1H-isoindole-1,3(2H)-dione

Reactivos

Ninguno

Disolventes

CCCCCC
Hexane

Condiciones de reacción

Condiciones detalladas
See reaction.notes.procedure_details.

Procedimiento

By using 2-[2,2,4,6,7-pentamethyl-3-(4-methylphenyl)-2,3-dihydro-1-benzofuran-5-yl]-1H-isoindole-1,3(2H)-dione, the title compound was synthesized according to Example 2a. Yield: 46%. Melting point: 141-143° C. (Hexane)

Fuente

DOI: 10.6084/m9.figshare.5104873.v1Patente: US07456162B2uspto-grants-2008_11