Reacción #348014

Ecuación de reacción

indole-3-carboxylic acid

1-bromononane

potassium carbonate

→

nonyl indole-3-carboxylate

Disolventes

N,N-dimethylformamide

Condiciones de reacción

Tratamiento posterior

1. 1
   FiltraciónAfter insoluble materials were filtered off
2. 2
   workup.ADDITIONthe filtrate was diluted with ethyl acetate
3. 3
   Lavadowashed with water and brine
4. 4
   Secadodried over magnesium sulfate
5. 5
   Concentraciónconcentrated
6. 6
   OtroThe solid was collected
7. 7
   Lavadowashed with hexane

Procedimiento

A mixture of indole-3-carboxylic acid, 1-bromononane and potassium carbonate in N,N-dimethylformamide was stirred at room temperature for 15 hours. After insoluble materials were filtered off, the filtrate was diluted with ethyl acetate, washed with water and brine, dried over magnesium sulfate and concentrated. The solid was collected and washed with hexane to give nonyl indole-3-carboxylate.

Fuente