Reacción #336827

ord-5056561b5b1446f29b22219556fed246

Ecuación de reacción

CCCCCCCCCCCCO
1-dodecanol
CCOC(=O)C(C)O
ethyl lactate
CCCCCCCCCCCCOC(=O)C(C)O
lauryl lactate
Rendimiento 80.0%

Reactivos

Ninguno

Condiciones de reacción

Temperatura
60°CELSIUS
Condiciones detalladas
See reaction.notes.procedure_details.

Procedimiento

A mixture of Novozym® 435 (1 kg), 1-dodecanol (4000 mL), and ethyl lactate (4000 mL) in a 50 L reactor was stirred (˜200 rpm) at 60±5° C. for 28 hours. Upon work-up, 4000 g of lauryl lactate (80% yield) was obtained as a pale yellow liquid. The purity of the product was >97% as assessed by GC.

Fuente

DOI: 10.6084/m9.figshare.5104873.v1Patente: US07863025B2uspto-grants-2011_01