Reacción #335366

ord-f1295af546364bb69de4497039d07db0

Ecuación de reacción

ClCC=C(Cl)Cl
3,3-dichloroallyl chloride
CC(C(=O)O)c1ccc2cc(O)ccc2c1
racemic 6-hydroxy-α-methyl-2-naphthaleneacetic acid
→
CC(C(=O)O)c1ccc2cc(OCC=C(Cl)Cl)ccc2c1
title compound
CC(C(=O)O)c1ccc2cc(OCC=C(Cl)Cl)ccc2c1
α-Methyl-6-(3,3-dichloroallyloxy)-2-naphthaleneacetic acid

Reactantes

ClCC=C(Cl)Cl
3,3-dichloroallyl chloride
CC(C(=O)O)c1ccc2cc(O)ccc2c1
racemic 6-hydroxy-α-methyl-2-naphthaleneacetic acid

Reactivos

Ninguno

Condiciones de reacción

Condiciones detalladas
See reaction.notes.procedure_details.

Tratamiento posterior

  1. 1
    OtroWhite crystals are obtained

Procedimiento

The title compound is prepared according to the method of Example 7 using 3,3-dichloroallyl chloride and racemic 6-hydroxy-α-methyl-2-naphthaleneacetic acid. White crystals are obtained having a melting point of 107°-109° C.

Fuente

DOI: 10.6084/m9.figshare.5104873.v1Patente: US05208344uspto-grants-1993_05