Reacción #334978

Ecuación de reacción

n-decyl alcohol

naphthalene-2,6-dicarboxylic acid dichloride

triethylamine

dimethylaminopyridine

→

titled compound

Rendimiento 56.3%

2-n-decyloxycarbonylnaphthalene-6-carboxylic acid chloride

Rendimiento 56.3%

Disolventes

methylene chloride

Condiciones de reacción

Tratamiento posterior

1. 1
   workup.DISTILLATIONthe solution was distilled
2. 2
   Otroto remove the solvent

Procedimiento

After a solution of n-decyl alcohol (0.5 g), naphthalene-2,6-dicarboxylic acid dichloride (0.6 g), and triethylamine (0.27 g) and a very small amount of dimethylaminopyridine in methylene chloride (50 ml) was stirred at room temperature overnight, the solution was distilled to remove the solvent, until the titled compound (about 0.5 g) was obtained.

Fuente