Reacción #324626

ord-e4989bf4efff40cca74e691b42b4316a

Ecuación de reacción

Cc1cc(O)cc(C)c1Br
4-bromo-3,5-dimethylphenol
Cc1ccc(S(=O)(=O)OCCC(C)(C)O)cc1
3-hydroxy-3-methylbutyl 4-methylbenzenesulfonate
Cc1cc(OCCC(C)(C)O)cc(C)c1Br
title compound
Cc1cc(OCCC(C)(C)O)cc(C)c1Br
4-(4-Bromo-3,5-dimethylphenoxy)-2-methylbutan-2-ol

Condiciones de reacción

Condiciones detalladas
See reaction.notes.procedure_details.

Procedimiento

The title compound is prepared from 4-bromo-3,5-dimethylphenol and 3-hydroxy-3-methylbutyl 4-methylbenzenesulfonate following a procedure analogous to that described in Step 3 of Intermediate 2. LC (method 1): tR=1.35 min; Mass spectrum (ESI+): m/z=269 [M+H—H2O]+.

Fuente

DOI: 10.6084/m9.figshare.5104873.v1Patente: US08642585B2uspto-grants-2014_02