Reacción #324358

Ecuación de reacción

aniline

propane sultone

→

3-phenylammonio-1-propanesulfonate

Rendimiento 95.0%

Disolventes

acetonitrile

Condiciones de reacción

Tratamiento posterior

1. 1
   Filtraciónthe solid of 3-phenylammonio-1-propanesulfonate was filtered
2. 2
   Otroair-dried

Procedimiento

A mixture of aniline (7 mmol) and propane sultone (10 mmol) was heated in 10 mL of acetonitrile at 12.0-130° C. for 9 h in a pressure tube under argon atmosphere. The product was allowed to cool to room temperature and the solid of 3-phenylammonio-1-propanesulfonate was filtered and air-dried. Yield: 95%.

Fuente