Reacción #313089

ord-91ad8c52c923465bb6c8f6d690e8f927

Ecuación de reacción

c1cnc2[nH]ccc2c1
7-azaindole
Cc1c[nH]c2ccccc12
3-methylindole
→
Cn1ccc2cccnc21
title compound
Rendimiento 58.0%
Cn1ccc2cccnc21
1-Methyl-1H-pyrrolo[2,3-b]pyridine
Rendimiento 58.0%

Reactantes

—
40(a)
c1cnc2[nH]ccc2c1
7-azaindole
Cc1c[nH]c2ccccc12
3-methylindole

Reactivos

Ninguno

Condiciones de reacción

Condiciones detalladas
See reaction.notes.procedure_details.

Procedimiento

According to the procedure of Preparation 40(a), except substituting 7-azaindole (2.28 g, 1.83 mmole) for the 3-methylindole, the title compound (1.4 g, 58%) was prepared as a yellow oil: MS (ES) m/e 133 (M+H)+.

Fuente

DOI: 10.6084/m9.figshare.5104873.v1Patente: US07557125B2uspto-grants-2009_07