Reacción #312607
ord-b03a5db651ec40d3bbfb5d7f0db51248
Ecuación de reacción
t-butyl 4-(1-benzenesulfonyl-1H-indol-4-yl)piperazine-1-carboxylate
HCl
→
title product
Rendimiento 99.0%
1-(Phenylsulfonyl)-4-piperazin-1-yl-1H-indole Hydrochloride
Rendimiento 99.0%
Reactivos
Ninguno
Disolventes
Condiciones de reacción
Condiciones detalladas
See reaction.notes.procedure_details.
Tratamiento posterior
- 1Filtraciónfiltered
- 2OtroThe filtercake is dried
Procedimiento
A portion of the t-butyl 4-(1-benzenesulfonyl-1H-indol-4-yl)piperazine-1-carboxylate (0.85 g) is stirred in a mixture of 4N HCl and dioxane at room temperature for 2 hrs and filtered. The filtercake is dried to give the title product as a while solid, 0.64 g (99% yield) mp 60° C. identified by mass spectral and NMR analyses.