Reacción #312238

Ecuación de reacción

caprolactam

o-aminothiophenol

p-toluenesulfonic acid

→

2-(5-aminopentyl)benzothiazole

Condiciones de reacción

Tratamiento posterior

1. 1
   Otrowhile removing water
2. 2
   workup.DISTILLATIONby distillation

Procedimiento

A mixture of caprolactam (62 g; 0.55 mole) and o-aminothiophenol (68.8; 0.55 mole) was heated with p-toluenesulfonic acid (4.3 g) at 190°-260° for 41/2 hrs. while removing water by distillation. The product was essentially pure 2-(5-aminopentyl)benzothiazole.

Fuente