Reacción #302879

ord-480eeee1e94949eab8564a608a63afe1

Ecuación de reacción

[Cl-].[Cl-].[Mg+2]
magnesium chloride
C[CH2][K].O=C(O)CC(=O)O
ethyl potassium malonate
→
O=C([O-])CC(=O)[O-].[CH2]C.[Mg+2]
Ethyl Magnesium Malonate

Reactantes

[Cl-].[Cl-].[Mg+2]
magnesium chloride
C[CH2][K].O=C(O)CC(=O)O
ethyl potassium malonate

Reactivos

Ninguno

Disolventes

CC(C)O
isopropanol

Condiciones de reacción

Condiciones detalladas
See reaction.notes.procedure_details.

Tratamiento posterior

  1. 1
    FiltraciónAfter filtration, ethyl magnesium malonate
  2. 2
    Otrowas dried in vacuo

Procedimiento

To a stirred aqueous solution of 1.5 M magnesium chloride and 3 M ethyl potassium malonate was added five volumes of isopropanol. After filtration, ethyl magnesium malonate was dried in vacuo.

Fuente

DOI: 10.6084/m9.figshare.5104873.v1Patente: US08192952B2uspto-grants-2012_06